@Research Paper
<#LINE#>Vapour phase isomerisation of ortho-toluidine over modified supported V-Mo oxide catalysts: Influence of process parameters and metal loadings on catalytic and thermodynamic properties<#LINE#>Neha@Marghade,V.R.@Chumbhale,A.K.@Goswami<#LINE#>1-7<#LINE#>1.ISCA-RJCS-2015-039.pdf<#LINE#>University Institute of Chemical Technology, North Maharashtra University, Jalgaon, 425001, INDIA @ Catalysis and Inorganic Chemistry Division, CSIR-National Chemical Laboratory, Pune- 411008, INDIA <#LINE#>13/3/2015<#LINE#>9/6/2015<#LINE#>The vapour phase transformation of o-toluidine isomerisation has been studied over modified V-MO catalyst at different process parameters. The objective of this work is to evaluate the catalytic performance of modified V-MO catalyst carried out by impregnation method with acidic metal salts of Boron and Phosphorus qualitatively and quantitatively also with Mg doped catalyst and compare with parent supported V-Mo catalyst as well as modified catalyst obtained by Mg doping. Catalytic properties (conversion, selectivity) and thermodynamic properties (The Arrhenius activation energy, enthalpy, entropy and Gibbs’s free energy) are compared at ambient pressure and at identical reaction parameters using down-flow fixed bed reactor. Catalysts are characterized by x-ray diffractometry for any new phase formation and were ascertained by JCPDS diffraction files. The role of new phase (s) formation in the title reaction is justified.  <#LINE#> @ @ Industrial organic chemistry, VCH New York, 376(1997) @No $ @ @ Weisermal K. and Aree H.J., In: IndustriChemistry ,Verlag Chemie, 329, (1978) @No $ @ @ Hans-Jiirgen Arpe, Frankfurt am Main andWiesbaden, Process for the manufacture of Oand/or m-toluidine And/ or p-toluidine, Patent Number4, 554, 380 Date of Patent: * Nov. 19, (1985) @No $ @ @ Juarez Lopez R., Godjayeva N.S. , Cartes CarberanFierro J.L.G. and Mamedov F.M., Oxidative dehydrogenation of ethane on supported vanadium containing oxides, Applies Catalysis A:G @No $ @ @ Chaudhari S.M., Waghulde A.S., Samuel V., Bari M.L. and Chumbhale V.R., Characterization of ZnO and modified ZnO catalysts for anaerobic oxidation of cyclohexanol, Res J.chem.sci,3(7), 38-44(2013) @No $ @ @Kabir Homayum, Chowdhari Samiul Islam and Hasan Tariqul, Synthesis and characterization of Mono and Diarma-halo esters as a Initiator for H2 oxidation,Res.J.chem.sci., 2(6),50-54(2012) @No $ @ @ Gupta Y.K., Agrawal S.C., Madnawat S.P.and Ram Narain, Synthesis and characterization and antimicrobial studies of some Transition Metal complexes of Schiff  68-71 (2012) @No $ @ @ Sonawane Vilas Y., Mechanistic study of chromium(VI) catalysed oxidation benzylalcohol by polymer supported Res J. chem.Sci,1(1), 25-30 (2011) @No $ @ @ Anand R.,  Maheswari R., Agashe M., .Chumbhale V. R., and Rao B. S., A compararative study of ortho-toluidine isomerisation over medium and large pore zeolite, Bulletine of the catalysis society of India 1 (2000) @No $ @ @ Chumbhale V.R., Pardhy S.A., Anilkumar M., Kadam S.T. and Bokade V.V., Vapor phase oxidation of acetophenone to benzoic acid over binary oxides of V Chemical Egg. Research and Design, 83(A), 75-80 @No
<#LINE#>A Novel Bromonaphthyl Based 2-Amino-1,3-Thiazines: Synthesis, Characterization with Invitro Antimicrobial Screening<#LINE#>Prakash@N,Sivagami@S,N@Ingarsal<#LINE#>8-11<#LINE#>2.ISCA-RJCS-2015-085.pdf<#LINE#>PG and Research Department of Chemistry, Rajah Serfoji Govt. College, Thanjavur-613 005, Tamilnadu, INDIA<#LINE#>16/6/2015<#LINE#>23/6/2015<#LINE#>A clinically important substrate of bromosubstituted acetylnaphthalene was used as the precursor for the preparation of a series  of  1-(2-bromonaphthalen-6-yl)-3-phenylprop-2-en-1-ones. The formed unsaturated ketones on treatment with thiourea in the presence of base like KOH in alcohol yields corresponding 4-(2-bromonaphthalen-6-yl)-6-phenyl-6H-1,3-thiazin-2-amine. The synthesized thiazines are evaluated their structure on the basis of NMR, MASS, IR and Elemental analyses along with their physical data. The antibacterial and antifungal activities indicate some of these thiazines are potential antimicrobial agents.  <#LINE#> @ @ Saranya A.V., Ravi S and Venkatachalapathi S., Invitro antioxidant activity of diethyl malonate adducts of phenothiazine, Res. J. Chem. Sci.,), 82-85 (2013) @No $ @ @ Koketsu M., Tanaka K., Takenaka Y., Kwong C.D. and Ishihara H., Synthesis of 1,3-thiazine derivatives and their evaluation as potential antimycobacterial agents,Eur. J. Pharm. Sci.,15307-310 (2002) @No $ @ @Bozsing D., Sohar P., Gigler G. and Kovacs G.,  Synthesis and pharmacological study of new 3, 4-dihydro-2H, 6H-pyrimido-[2, 1-b][1, 3] thiazines, Eur. J. Med. Chem.,31, 663-668 (1996) @No $ @ @ Florio S. and Leng J.L., Synthesis and reactivity of 4-substituted-2,3-dihydrobenzo-1,4-thiazines, J. Het. Chem.,19, 237-240 (1982) @No $ @ @ Suarez M., Novoa H., Verdecia Y., Ochoa E., Alvarez A., Roberto R.,Alvarez M., Dolores M., Seoane C., Norbert M.B., Oswald M.P., Nazario M., A straight forward synthesis and structure of unprecedented iminium salts of dihydropyrido[3,2-E][1,3]thiazines, Tetrahedron,62, 1365-1371 (2006) @No $ @ @ Christophersen C., Secondary metabolites from marine bryozoans, Acta Chem. Scand., 69, 517-529 (1985) @No $ @ @ Rathore M.M., Parhate V.V. and  Rajput P.R., synthesis and antimicrobial activities of some bromo-substituted 1,3-thiazines,  Int. J. Res. Pharm and Biomed. Sci., , 59-62 (2013) @No $ @ @ Bhanat K., Parashar B and Sharma V.K., Microwave induced synthesis and antimicrobial activities of various substituted pyrazolidines from chalcones, Res. J. Chem. Sci.,4(2), 68-74 (2014) @No $ @ @ Bhale P.S., Dongare S.B. and Chanshetti U.B., Synthesis and antimicrobial screening of chalcones containing imidazo[1,2-a]pyridine nucleus, Res. J. Chem. Sci.,3(12), 38-42 (2013) @No $ @ @ O'Brien P.J., Molecular mechanisms of quinone cytotoxicity, Chem. Biol. Interact,80(1), 1-4 (1991) @No $ @ @ Ruy C.K., Choi K.U., Shim J.Y., You H.J., Choi I.H. and Chae M., Synthesis and antifungal activity of 6-arylthio-/6-arylamino-4,7-dioxobenzothiazoles, Bio org. Med. Chem., 11(18), 4003-4008 (2003) @No $ @ @ Girdler R.B., Gore P.H. and Hoskins J.A., A re-examination of the Friedel–Crafts acetylation of 2-bromonaphthalene, J. Chem. Soc.(C) 518-520, (1966) @No 
<#LINE#>Synthesis and Characterization of Polydentate macrocyclic Schiff bases (14-membered atoms) and their complexes with Co (II), Ni (II), Cu (II) and Zn (II) ions<#LINE#>A.A@Mohammed,A.M.@Al-Daher,H.A.@Mohamad,R.G.@Harrison<#LINE#>12-19<#LINE#>3.ISCA-RJCS-2015-086.pdf<#LINE#>Department of Chemistry, College of Science, University of Mosul, Mosul, IRAQ @ Department of Chemistry, College of Education, University of Salahaddin, Erbil, IRAQ @ Department of Chemistry and Biochemistry, Brigham Young University, Provo, Utah 84602, USA<#LINE#>17/6/2015<#LINE#>28/6/2015<#LINE#>The condensation reactions of [2+2] carbohydrazide or thiocarbohydrazide with 3,4-hexanedione in a (1:1) molar ratio in aqueous solution at room temperature resulted in the formation of the novel Schiff bases tetraimine, macrocyclic ligands (L) : 2,3,9,10-Tetraethyl-6,13-dione-1,4,5,7,8,11,12,14-octaaza-cyclotetradeca-1,3,8,10-tetraene and (L):2,3,9,10-Tetraethyl– 6,13 –dithione-1,4,5,7,8,11,12,14-octaaza-cyclotetradeca-1,3,8,10-tetraene. Mononuclear complexes with the compositions [Co(L)Cl]. 3HO; [M(L)] Cl.nH (M = Ni (II), Cu (II) or Zn (II); n = 0 when M = Zn (II) and n = 3 when M = Ni (II) or Cu(II)) ; [M(L)Cl]. nH; (M=Co (II), Ni (II) or Cu (II); n=0 when M=Ni (II) and n=2 when M= Co (II) or Cu (II)); and also [Zn(L] Cl.HO were obtained by reacting metal (II) chlorides with the ligand (L)  or (L) in (1:1) molar ratio in ethanol. Mass and infrared spectral techniques suggest the structural features of 14-membered [2+2] Schiff base macrocyclic ligands while the nature of bonding and the stereochemistry of the complexes have been deduced by elemental contents analyses molar conductivity and magnetic susceptibility measurements, IR, MS and electronic spectral studies. The magnetic moments and electronic spectral data suggested a coordination number six (octahedral geometry) for the [Co(L)Cl]. 3HO; [M(L)] Cl.nH and [Zn(L] Cl.HO complexes while the [M(L)Cl]. nH; are of four coordinated geometry (tetrahedral). <#LINE#> @ @ Buttrus N.H, Ahmed S.A. and Jameel W.M., Synthesis and characterization of homo and hetero dinuclear and trinuclear Co(II), Ni (II),Cu(II) and Zn(II) complexes with 26 – membered N donor  macrocyclic ligand, Res. J. Chem . Sci , 3(11), 47-54 (2013) @No $ @ @ El-Gammal O.A., Bekheit M.M. and El-Brashy S.A, Synthesis, characterization and in vitro antimicrobial studies of Co (II), Ni (II) and Cu (II) complexes derived from macrocyclic compartmental ligand, Spectrochim. Acta A, 137, 207–219 (2015) @No $ @ @ Moi M.K., Meares C.F., McCall M.J., Cole W.C. and Denardo S.J., Copper chelates as probes of biological systems: Stable copper complexes with a macrocyclicbifunctional chelating agent, Anal. 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Stru., 1019, 135–142 (2012) @No $ @ @ Krishna E.R., Reddy P.M., Sarangapani M., Hanmanthu G., Geeta B. and Rani K.S., Synthesis of  donor macrocylic Shiff base ligands and their Ru (II), Pd (II) Pt (II) metal complexes for biological studies and catalytic oxidation of didanosine in pharmaceuticals, Spectrochim. Acta A , 97, 189-196 (2012) @No $ @ @ Asuero A.G., Schiff bases derived from biacetyl as analytical reagents: A review, microchem. J., 26, 527–556 (1981) @No $ @ @ Muzammil K., Trivedi P. and Khetani D.B., Synthesis and Characterization of Schiff base m- nitroaniline and their complexes, Res. J. Chem. Sci., 5(5), 52-55 (2015) @No $ @ @ Singh D.P., Kumar K. and Sharma C., Synthesis, Characterization, and antimicrobial activities of macrocyclic complexes of divalent transition metal ions, Synth. React. Inorg., Met. –Org. Nano Met. 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A., Spectral, magnetic, thermal and electrochemical studies on new copper (II) thiosemicarboazone complexes, J. Coord. Chem, 58(8), 713–733 (2005) @No $ @ @ Karekal M.R. and Mathada M.B.H., Synthesis, characterization and biological screening of binuclear transition metal complexes of biocompartmental Schiff bases containing indole and resorcinol moieties and D  (), Turk. J. Chem. , 37, 775 – 795 (2013) @No $ @ @ Khan T.A., Naseem S., Hajra R. and Shakir M., Synthesis, physicochemical, and antimicrobial screening studies of complexes of Co (II), Ni (II), Cu (II) and Zn (II) with 18 – membered Schiff base Octaazamacrocyclic ligand, Synth. React. Inorg. Met. – Org. Nano Met. Chem., 40 , 861 -868  (2010) @No $ @ @ Buttrus N.S., Synthesis and characterization of some Cr+3, Fe+3, Co+2, Ni+2Cu+2 and Zn+2 complexes with N-phthalyl amino acid ligands, Res. J. Chem. 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<#LINE#>Synthesis, Characterization and Antimicrobial screening of some Azo compounds derived from Ethyl vanillin<#LINE#>S.K.@Pagariya,R.M.@Pathade,P.S.@Bodkhe<#LINE#>20-28<#LINE#>4.ISCA-RJCS-2015-088.pdf<#LINE#> Department of Chemistry, Vidyabharati Mahavidyalaya, Amravati, 444602, INDIA<#LINE#>19/6/2015<#LINE#>30/6/2015<#LINE#>Azo compounds were synthesized in excellent yield by diazotization of some substituted aromatic amines using NaNO and concentrated HCl followed by coupling with ethyl vanillin in alkaline medium. These azo compounds were characterized by FTIR and H1 NMR spectroscopic technique and have been tested against the growth of five gram positive and negative microorganisms in order to assess their antimicrobial activity. <#LINE#> @ @ Towns A.D., Developments in azo disperse dyes derived from heterocyclic diazo compounds, Dyes and Pigments, 42, 3-28 (1999) @No $ @ @ Zollinger H., Synthesis, properties and applications of organic dyes and pigments, Color Chemistry, third revised edition,Wiley-VCH.,Weinheim (2003) @No $ @ @ Gayatri C. and Ramalingam A.,Z-scan determination of the third order optical nonlinerities of an azo dye using dipole: pumped Nd:Yag laser, Optik, 119(9), 409-414 (2008) @No $ @ @ Sakong C., Kim Y. D., Choi J. H., Yoon C. and Kim J.P., The synthesis of thermally stable red dyes for LCD color filters and analysis of their aggregation and spectral properties, Dyes and Pigments, 88(2),166-173 (2011) @No $ @ @ Bae J.S., Freeman H.S. and El-Shafei A., Metallization of non-genotoxic direct dyes, Dyes and Pigments, 57(2), 121-129 (2003) @No $ @ @ Sanjay F.T., Dinesh M.P., Manish P.P. and Ranjan G.P., Synthesis and antibacterial activity of novel pyraazolo [3,4-b] quinoline base heterocyclic azo compounds and their dyeing performance, Saudi Pharm. Journal, 15(1), 48-54 (2007) @No $ @ @ Child R.G., Wilkinson R.G. and Tomcu-Fucik A., Effect of substrate orientation of adhesion of polymer joints, Chem. Abstr., 87, 6031 (1977) @No $ @ @ Garg H.G. and Prakash C.J., Preparation of 4-arylazo-3,5-disubstituted-(2H)-1,2,6-thiadizine1,1-dioxides, Med. Chem.,15(4), 435-436 (1972) @No $ @ @ Koshti S.M., Sonar J.P., Sonawane A.E., Pawar Y.A., Nagle P.S., Mahulikar P.P. and More D.H., Synthesis of azo compounds containing thymol moiety, Indian J. Chem., 47B, 329-331 (2008) @No $ @ @ Pathan R.U. and Borul S.B., Synthesis and antimicrobial activity of azo compounds containing drug moiety,Oriental J. Chem., 24(3), 1147-1148 (2008) @No $ @ @ Rathod K.M., Synthesis and antimicrobial activity of azo compounds containing paracetamol moiety, Oriental J. Chem., 26(3), 1163-1166 (2010) @No $ @ @ Rathod K.M. and Thakare N.S., Synthesis and antimicrobial activity of azo compounds containing m-cresol moiety, Chem. Sci.Trans., 2 (1), 25-28 (2013) @No $ @ @ Rathod K.M., Synthesis and antimicrobial activity of azo compounds containing resorcinol moiety, Asian J. Research Chem., 4(5), 734-736 (2011) @No $ @ @ Pagariya R.F., Rathod K.M. and Thakare N.S., Synthesis, characterization and antibacterial screening of azo compounds containing vanillin moiety, Asian J. Research  Chem., 6(9), 824-827 (2013) @No $ @ @ Dahake P.R. and Kamble S.I., Investigatory study on antimicrobial activity and phytochemical screening of Butea monosperma Linn, BBRA, 11(3), 1695-1698 (2014) @No $ @ @ Alzoreky N.S. and Nakahara K., Antimicrobial activity of extracts from some edible plants commonly consumed in Asia, Int. J. Food Microbial, 80, 223-230 (2003) @No 
<#LINE#>Variation in Physico-chemical Characteristics of Water Quality of Bhindawas Wetland, Jhajjar, Haryana, India<#LINE#>Sunil@Kumar,Rajesh@Dhankhar<#LINE#>29-34<#LINE#>5.ISCA-RJCS-2015-089.pdf<#LINE#> Department of Environmental Sciences, Maharshi Dayanand University, Rohtak-124001, Haryana, INDIA<#LINE#>19/6/2015<#LINE#>27/6/2015<#LINE#>Present study was carried out to find spatial and temporal variation in the water quality of Bhindawas wetland and its recipient drain No. 8 at two month intervals over one year period from July 2010 to may 2011. Total nine sampling sites were selected from the study area. Seven sites selected from various parts of wetland, including wetland inlet and outlet. In addition, two sites were selected from drain no.8, which is adjacent to a wetland and a recipient of wetland outlet water. Range of pH, temperature, electrical conductivity, total dissolved solids, total suspended solids and turbidity varied from 6.45-8.26, 14-35.4ºC, 216-1963 µmho/cm, 142-1282 mg/l, 7.8-94mg/l and 4-62 NTU, respectively. Cationic concentration, viz. sodium, potassium, calcium and magnesium varied from 16-102, 2-63, 14-131 and 4-60 mg/l, respectively. Whereas, anionic concentration, viz. bicarbonate, chloride and sulphate varied from 48-666, 9-199 and 25-187 mg/l, respectively. Variation in dissolved oxygen was from 2.8 to 8.6 mg/l. Variation in total phosphorus, ammonia, nitrate, total alkalinity and total hardness were in the range of from below detection limit (BDL)-0.99, BDL-0.69, BDL-2.04, 40-576 and 54-576 mg/l, respectively. Heavy metals like copper, nickel, lead and total chromium were found below detection limit (BDL). <#LINE#> @ @ Abir S., Seasonal variations in physico-chemical characteristics of Rudrasagar wetland: A Ramsar site, Tripura, North East, India, Res. J. Chem. Sci., 4(1), 31-40 (2014) @No $ @ @ Deshmukh K.K.,  Assessment of groundwater quality and its impact on human health from Sangamner Area, Ahmednagar District, Maharashtra, India, Internt JRes. Chem. Env., 4(3), 40-48 (2014) @No $ @ @ Eliska R.M. and Kimberly E., Wetland ecosystem changes after three years of phosphorus addition, Wetlands, 28, 914–927 (2008) @No $ @ @ Beman J.M., Arrigo K.R and Matson P.A, Agricultural runoff fuels large phytoplankton blooms in vulnerable areas of the ocean, Nat., 434, 211–214 ( 2005) @No $ @ @ Binhe G. and Thomas D., Effects of Plant Community and Phosphorus loading rate on constructed wetland performance in Florida, USA,  Wetlands, 28, 81–91 (2008) @No $ @ @ Covney M.F., Stites D.L., Lowe E.F., Battow L.E. and Conrow R., Nutrient removal from eutrophic lake water by wetland filtration, Ecol. 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Sci.,5(5), 24-26 (2015) @No $ @ @ Chincihilla L.M., Gonzale E. and Comin F.A., Assessing metals pollution in ponds constructed for controlling runoff from reclaimed coal mines, Environ. Monit. Assess.,186, 5247-5259 (2014) @No $ @ @ Chinna, R.P. and Gundala P. H., Analysis of Water Quality Parameters of Lakshmipuram tank, Anantapuramu (d), Andhra Pradesh, India, J. of Chem. Sci.,5(4), 26-32 (2015) @No $ @ @ Singh, V.B., Piplode S., Thakur V. and Agrawal R., Comparative Physico-Chemical Analysis of Narmada River Water at Barwani and Khalghat, MP, India, Res. J. of Chem. Sci.,5(3), 6-8 (2015) @No $ @ @ Bodane A.K., Physico-Chemical Analysis of Some Dam Water Samples of Lakhundar Dam of Palsawad Son, District-Shajapur, MP, Res. J. of Chem. Sci.,5(4), 45-48 (2015) @No $ @ @ APHA: Standard Methods for the Examination of Water and Wastewater, 21st Edn. 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GeoSci.,, 599-609 (2010) @No $ @ @ Horne A.J. and Goldman C.R., Limnology, McGraw-Hill, Inc., New York, NY (1994) @No $ @ @ Cole G., Textbook of Limnology, Waveland Press, Inc., Prospect Heights, IL., 412 (1994) @No $ @ @ US DHEM: Drinking wáter standards-1962, Washington, DC, US Department of Health, Education and Welfare, Public Health Services, US Goverment Printing Office, Publication No., 956 (1962) @No $ @ @ Chakraborty A., Padmavati G. and Ghosh A.K., Tidal variation of phytoplankton in the coastal waters of South Andaman, India, J. Environ. Biol.,36, 207-214 (2015) @No $ @ @ Kim J.B., Hong S., Lee W., Lee Y., Kim H.C. and Cho Y., Evaluation of phytoplankton community composition in the eutrophic Masan Bay by HPLC pigment analysis, J. Env. Biol.,36, 491-498 (2015) @No $ @ @ Smith V.H., Tilman G.D.  and Nekola J.C., Eutrophication: impacts of excess nutrient inputs on freshwater, marine, and terrestrial ecosystems, Environ. Pollut., 100179–196 (1999) @No $ @ @ Wetzel R.G., Limnology of Lake and River Ecosystems. Third Edition. Academic Press,San Diego, CA, 1006 (2001) @No $ @ @ Keshin T.E., Nitrate and heavy metal pollution resulting from agricultural activity: A case study from Eskipazar (Karabuk,Turkey), Environ. Earth Sci.,61, 703-721 (2010) @No $ @ @ Puttaiah E.T. and Kiran B.R., Heavy metal transport in a sewage fed lake of Karnatala, India, 12th world lake conference, 347-354 (2008) @No $ @ @ Ahmad Z., Khalid A., Al-Ghanim H.F.A. Al-Balawi F. Al-Misned S. Maboob and Suliman E.M., Accumulation of heavy metals in the fish, Oreochromis niloticus and Poecilia latipinna and their concentration in water and sediment of dam lake of Wadi Namar, Saudi Arabia, J. Env. Biol.,36, 295-299 (2015) @No
<#LINE#>Qualitative analysis of 5th Generation of Carbapenem Antibiotics by UV Spectrophotometric Method<#LINE#>Shalvi@Sharma,Nitasha@Agrawal,Jaskaran@Singh,S.K.@Shukla<#LINE#>35-39<#LINE#>6.ISCA-RJCS-2015-090.pdf<#LINE#> Amity institute of Forensic Sciences, Amity University, Noida, U.P 201301, INDIA<#LINE#>24/6/2015<#LINE#>7/7/2015<#LINE#>In the present study the Quantitative analysis of 5th generation Carbapenems viz. Meropenem and Imipenem was done. They are used in case of severe infections like: infection in urinary tract, respiratory tract, etc.as they have broad spectrum of activities can be able to work on gram positive, gram negative as well as aerobics and anaerobic bacteria’s. For analysis of both antibiotics we took two samples from each Meropenem and Imipenem named as 1stControl i.e. Pharmaceutical formulation 2nd was extracted which was extracted from Synthetic urine. Here, UV spectrophotometer was used for the estimation of meropenem and imipenem in pharmaceutical formulations. The  max for both the samples were estimated with meropenem having 305nm while imipenem having 295nm. At this wavelength extracted sample absorbance was observed. Similarly, %amount of extracted antibiotics from urine sample was also calculated. As it is usually not used in criminal activities till now, overdosing symptoms can be possible. As most of the elimination is by kidney so urine sample are used for analysis. Here quantitative analysis was done as at what amount these antibiotics can be detected in both standard as well as in synthetic urine by UV spectrophotometry.  <#LINE#> @ @ Tripathi K.D., Essentials of Medical Pharmacology, New Delhi, India, 390-404, (2013) @No $ @ @ Raghu Babu K., Aruna Kumari N. and Vijaya Lakshmi R., Spectrophotometric Determination of Doripenem, Ertapenem in Bulk and injection Formulation by F-C Reagent, International Journal of Pharmaceutical Sciences and Drug Research, 5(4) 184-86 (2013) @No $ @ @ Falagas E. Matthew, Panagiota Lourida, Panagiotis Poulikakos, Petros I. Rafailidis and Giannoula S. Tansarlia, Antibiotics treatment of Infections due to Carbapenem-Resistent Enterobacteriaceae: Systematic Evaluation of the Available Evidence American Society for Microbiology, Antimicrob. Agents Chemother, 58, 654-63 (2013) @No $ @ @ Tanveer begum N., Karthik Kumar B and Thiruvengadinrajan V.S., Analytical method development and validation of Lidocaine in ointment and formulation by UV Spectrophotometric method, International Journal of Pharmacy and Pharmaceutical Sciences, 4(2), 610-14 (2012) @No $ @ @ Shah A., Vaishali Sapna M., Rathod Rajesh, Parmar R. and Dushyant A.Shah, Development and Validation of analytical method for Meropenem in Pharmaceutical dosage form International Journal of Institutional Pharmacy and Life Sciences, 2249-6807, 503-09 (2012) @No $ @ @ Jayapraba1 S., Jerad  A suresh 2 and Niraimathi V., Forced oxidative degradation study of Doripenem by UV spectrophotometric method International Journal of Pharmacy and Pharmaceutical Sciences ISSN- 0975-1491, 5, 1 (2013) @No $ @ @ Zhang J, Musson DG, Birk KL, Cairns AM, Fisher AL, Neway W and Rogers JD, Direct injection HPLC assay for the determination of a new carbapenem antibiotics in human plasma and urine, J Pharm Biomed Anal., 1, 27(5), 755-70 (2002) @No $ @ @ Keiko Kameda et.al, HPLC method for measuring Meropenem and Biapenem concentration in Human peritoneal Fluid and Bile: Application to comparative pharmacokinetics investigations Journal of Chromatographic Science, 48 (2010) @No $ @ @ Judyta Cielecka-Piontek, Daria Szymanowska-Powa\nowska, Magdalena Paczkowska, Piotr 	ysakowski, Przemys\naw Zalewski and Piotr Garbacki Stability, Compatibility and Microbiology activity studies of Meropenem, clavulanate potassium The Journal of Antibiotics, 68,35–39 (2015) @No 
<#LINE#>Compositional analysis and Antimycobacterium Tuberculosis Activity of Essential Oil of Hyptis Suaveolens Lamiceae<#LINE#>M.@Runde,D.@Kubmarawa,Maina@H<#LINE#>40-44<#LINE#>7.ISCA-RJCS-2015-091.pdf<#LINE#> Department of Chemistry, School of Pure and Applied Science Modibbo Adama University of Technology P.M.B. 2076 Yola Adamawa State NIGERIA<#LINE#>30/6/2015<#LINE#>4/7/2015<#LINE#>Fresh leaves of Hyptis suaveolens were collected and pretreated for essential oil analysis with the sole aim of linking the ethnomedicinal uses of this plant by the people of Adamawa State Nigeria to its essential oil composition. The results obtained from the analysis shows that 68 compounds were present in varying concentration out of which 16 compounds have appreciable concentration making 75.135 % of the total abundance. The major compound being Caryophyllene (20.643 %) followed by Sabinene (16.711 %) and Terpinolene (8.490 %). The essential oil of Hyptis suaveolens also showed anti mycobacterium activity when tested on strain 7H9/ADC with MIC of 3.13 %. This activity was compared with standard drug Rifampicin which also has MIC of 0.1 µg/ml. <#LINE#> @ @ Kingston D.G., Rao. M.M. and Zucker W.V., Plant Anticancer against IX Constituent of Hyptis suaveolens, J. of Nat. pro.,42(5 496-499 (1997) @No $ @ @ The wealth of India (Raw materials), CSIR New Delhi., 5, 159 (1964) @No $ @ @ Kirtikar K.R. and Basu B.D., Indian Medicinal Plants, Singh B and Singh M.P. Publishers India., 3, 2032 (1991) @No $ @ @ Annie S., Rhadika S., Udupa A.L., Udupa S.L. and Somashekar S., Wound Healing Property of Ethanolic Extract of Leaves of Hyptis suaveolens with supportive role of Antioxidant Enzymes, Ind. J. of exp. Bio., 41(3),238-241 (2003) @No $ @ @ Chatterjee A. and Pakrashi S.C., The Treatise on Indian Medicinal Plants, PID, New Delhi: 5, 15 (1997) @No $ @ @ Chitra S., Patil M.B. and Ravi K., Wound Healing Activity of Hyptis suaveolens (L)Poit, Int. J. of Pharm. Tech. Res., 1(3), 737-744 (2009) @No $ @ @ Umedum N.L., Nwajagu U., Udeozo I.P., Anarado C.E. and Egwuatu C., The efficacy of Hyptis suaveolens: A review of its Nutritional and Medicinal Application, Eur. J. of Medi. Pl., 4(6) 661-674 (2014) @No $ @ @ Carson C.F. and Riley T.V., Antimicrobial Activity of a Major Component of the Essential oil of Melaleuca alternifolia. J. of App. Bacterio.,78(3), 264-269 (1995) @No $ @ @ Ramzi A.M., Mansour S.A., Mohammed A.A., Adnan J.A. and Jamal M.K., GC and GC/MS Analysis of Essential Oil Composition of the Endemic Soqotraen Leucas virgata Balf. f. and Its Antimicrobial and Antioxidant Activities. Int. J. Mol. Sci.,14(11), 23129-23139; doi:10.3390/ijms141123129 (2013) @No $ @ @ Giovanni B., Guido F., Angelo C., Illaria M., Pier L.C and Barbara C., Repellent of Hyptissuaveolens whole Essential oil and major Constituents against Adult of Granary weevil sitophilus granaries. Bullet. of insectol., 65(2), 177-183 (2012) @No $ @ @ Chatri M., Amri B. and Mansyurdin P.A., Chemical Components of Essential oils of the Leaves of Hyptis suaveolens  (L) poit from Indonesia, Amer. J. of Res. Comm.,2(10), 30-38 (2014) @No $ @ @ Sharma N., Verma U.K. and Tripatti A., Bioactivity of Essential oil from Hyptissuaveolens against Storage mycoflora. Proc. Inc. cont. Controlled Atmosphere and Fumigation in Stored Product, Gold-cast Austrilia. 8-13thFTIC Ltd. Publishing, Israel., 99-116 (2007) @No $ @ @ Okonogi S., Chansakaow S., Vejabhikul S., Tharavichikul P., Herphokanount J, Nakano A. and Ikegami F., Antimicrobial Activity and Pharmaceutical Development of Essential oil from Hyptis suaveolens. Proc. WOCAMP.,3(4), 163 (2005) @No $ @ @ Fun C.E and Baerheim A.S., The Essential oil of Hyptis suaveolens poit Grown on Aruba. 10. 1002/ffj.2730080306, available on linelibrary.wiley.com visited., 14-6-2015 (2006) @No $ @ @ Azevedo N.R., Campos I.F., Ferreira H.D., Portes T.A., Santos S.C. Seraphin J.C and Ferri P.H., Chemical Variability in the Essential oil of Hyptis suaveolens. U. S Nat. lib. of Med. Nat. Inst. of Health,57(5), 733-6 (2001) @No $ @ @ Koba K., Raymoud C., Millet J., Chaumout J.P. and Sanda K., Chemical Composition of Hyptis pectinataL.H. lanceolata poit H. Suaveolens L and H. spicigeraLam, Essential oil from Togo, J.of Essent.oil Bea. Pl.10(5), 357-364 (2007) @No $ @ @ Dorman H.J.D. and Deans S.G., Antimicrobial Agent from Plant: Antibacterial Activity of Plant Volatile oils, J. of App. Microbiol.,88, 308-316 (2000) @No 
<#LINE#>Compression ratio effect on Diesel Engine working with Biodiesel (JOME)-Diesel blend as fuel<#LINE#>P.@VenkateswaraRao<#LINE#>45-47<#LINE#>9.ISCA-RJCS-2015-095.pdf<#LINE#>Department of Mechanical Engineering, Kakatiya Institute of Technology and Science, Warangal- 506015, Telangana, INDIA<#LINE#>7/7/2015<#LINE#>11/7/2015<#LINE#>Continuous increase of energy demand in domestic and industrial sectors increases the pollution problems due to huge usage of fossil fuel. To overcome this problem it is necessary to develop an alternate and renewable source of energy which has less impact on environmental pollution. The wide varieties of plant based vegetable oils available are suitably converted to use in diesel engines as an alternative fuel. In this paper an attempt has been made to investigate the effect of compression ratio (CR) on performance characteristics of diesel engine with 20% Jatropha oil methyl ester (JOME) mixed with 80% diesel to form as B20D80 blend fuel (BF). Experiments were conducted on a variable compression ratio (VCR) engine at compression ratio of 14, 16, 18 and 20 for BF and at 14 and 20 for diesel fuel to compare the results. The performance parameters like brake thermal efficiency, BSFC, volumetric efficiency, CO, CO HC, NO and smoke intensity were measured and analyzed. It was observed that the increase in compression ratio, performance of engine increased appreciably with less BSFC for blend fuel. From the emission results, it was also observed that CO, HC, NO and smoke density reduces significantly but a slight increase in CO as the compression ratio increases. <#LINE#> @ @ Wijetunge R.S., Brace C.J., Hawley J.G., Vaughan N.D., Horrocks H.W. and Bird G.L., Dynamic behavior of a high speed direct injection diesel engine, SAE Paper No., 01-0829, (1999) @No $ @ @ He X. and Durrett R., Late intake closing as an emissions control strategy at tier 2 bin 5 engine-out NOx level, SAE Paper No., 01- 0637 (2008) @No $ @ @ Ramadhas A.S., Jayaraj S. and Muraleedharan C., Use of vegetable oils as IC engine fuels-a review, Renewable Energy, 29, 727–742 (2004) @No $ @ @ Szybist J., Song J., Alam M. and Boeham A., Biodiesel combustion, emissions and emission control, Fuel Processing Technol., 88, 679–691 (2007) @No $ @ @ Senthil Kumar M, Ramesh A and Nagalingam B, A comparison of the different methods to improve engine performance while using Jatropha oil as the primary fuel in a compression ignition engine, Intern. conference on Energy and Environmental Technol. for Sustain. Develop., 8-10, 267-274 (2003) @No $ @ @ Senthil Kumar M., Ramesh A. and Nagalingam B., Experimental Investigations on a Jatropha Oil Methanol Dual Fuel Engine, SAE Paper No., 01-0153, (2001) @No $ @ @ Muralidharan K., Vasudevan D., Sheeba K.N., Performance, emission and combustion           characteristics of biodiesel fuelled variable compression ratio engine, Energy, 36, 5385-5393 (2012) @No $ @ @ Gandure J and Ketlogetswe C, Marula Oil and Petrodiesel: A Comparative Performance Analysis on a Variable Compression Ignition Engine, Energy and Power Eng., 3(3), 339-342 (2011) @No $ @ @ Kannan T.K. and Marappan R., Study of Performance and Emission Characteristics of a Diesel Engine using Thevetia Peruviana Biodiesel with Diethyl Ether Blends, European J. of Scientific Res., 43, 563-570 (2010) @No $ @ @ Sundarapandian S. and Devaradjane G., Performance and Emission Analysis of Bio-Diesel Operated C I Engine, J. of Eng., Computing and Architecture, 1(2), 1-22 (2007) @No $ @ @ Pugazhvadivu M. and Sankaranarayanan G., Experimental Studies on a Diesel Engine Using Mahua Oil as fuel, Indian J. of Sci. and Technol, 787-791 (2010) @No $ @ @ Venkateswara Rao P.and Srinivasa Rao G., Production and Characterization of Jatropha Oil Methyl Ester, Intern. J. of Eng. Res., 2(2), 145-149 (2013) @No $ @ @ Okechukwu R.I., Iwuchukwu A.C. and Anuforo H.U., Production and Characterization of Biodiesel from Ricinus Communis Seeds,   Res. J. of Chem. Sci., 5(2), 1-3 (2015) @No 
<#LINE#>Physical characteristics, Chemical composition and Distribution of constituents of the Neem seeds (Azadirachta indica A. Juss) collected in Senegal<#LINE#>Djibril@Diedhiou,Mamadou@Faye,Gérard@Vilarem,CodouGeuye@Mar-Diop,@SockOumar,Luc@Rigal<#LINE#>52-58<#LINE#>10.ISCA-RJCS-2015-097.pdf<#LINE#>Laboratoire de Chimie Agro-Industrielle (LCA), ENSIACET, INP Toulouse, 4 Allée Emile Monso - BP 44362 -31030 Toulouse Cedex 4, FRANCE @ Laboratoire d’Electrochimie et des Procédés Membranaires (LEPM), Université Cheikh Anta Diop de Dakar, BP 5085 Dakar-fann, SENEGAL<#LINE#>8/7/2015<#LINE#>13/7/2015<#LINE#>Neem seeds (Azadirachta indica A. Juss) collected in southwest Senegal were characterized. The physical characterization revealed an average seed weight of 0.28 g with 50.89% of kernel and 49.11% of hull. These seeds contain 29.27±0.06% of lipids, 12.10±0.32% of proteins and 43.98±2.67% of parietal constituents (celluloses, hemicelluloses and lignins) with 30.33±1.12% of cellulose containing 68.96% of fibers. The study of the constituent(s) distribution showed that 96.82% of the lipids and 92.20% of the proteins are localized in the kernel, while 92.22% of the parietal constituents are localized in the hull. The azadirachtin is localized in the kernel (99.35%). Neem seeds also contain 14.99±0.37% of hydrosoluble, 0.11±0.05% of polyphenols and 0.76‰ of essential oil. The composition of the proteins revealed 17 amino acids with the predominant compound being glutamic acid (23.65%). The oil fatty acids are oleic acid (41.91±0.69%), linoleic acid (19.59±0.44%), stearic acid (18.71±0.46%) and palmitic acid (15.59 ± 0.27%). The oil is predominantly composed of unsaturated fatty acids (63% in the fatty acids composition). The oil is mainly composed of triglycerides (97.69%). These are mostly made up of SOL (52.93%) and POL (36.61%). The sterols being present at 2.04 g.kg-1 in the oil are mainly composed of -sitosterol, which represents 61.08% of the total sterols. The total tocopherol content is 33.87 mg. 100g-1 and the tocopherol is the major compound with 68.69% of total tocopherols. <#LINE#> @ @ Chopra I.C., Gupta K.C. and Nazir B.N., Preliminary study of antibacterial substance from Melia azadirachta, Indian J. Med. Research., 40, 511-515 (1952) @No $ @ @ Fortin D., Lô M. and Maymart G., Plantes médicinales du Sahel, ENDA Editions, Dakar (1997) @No $ @ @ Schmutterer H., The neem tree, Azadirachta indica A, Juss and other meliaceous plants, VCH: Weinheim 1995) @No $ @ @ Butterworth J.H. and Morgan F.D., Isolation of a substance that suppress feeding in locusts, J. Chem. Soc. Chem. Communs., 23-24 (1968) @No $ @ @ Kaura S.K., Gupta S.K. and Chowdhury J.B., Morphological and oil content variation in seeds of Azadirachta indica A, Juss. (Neem) from northern and western provenances of India, Plant Foods for Hum. Nutr., 52, 293-298 (1998) @No $ @ @ Sidhu O.P., Kumar V. and Behl H.M., Variability in neem (Azadirachta indica) with respect to azadirachtin content, J. Agric. Food Chem., , 910-915 (2003) @No $ @ @ Imam H., Hussain A. and Ajij A., Neem (Azadirachta indica A. Juss): A Nature's Drugstore: An overview, ISCA International Res, J. Biol. Sci., 1(6), 76-79 (2012) @No $ @ @ Luo X., Ma Y., Wu S. and Wu D., Two novel azadirachtin derivatives from Azadirachta indica, J. Nat. Prod., 62, 1022-1024 (1999) @No $ @ @ Djenontin T.S., Wotto V.D., Avlessi F., Lozano P., Dominique K.C., Sohounhloué D.K.C. and Pioch D., Composition of Azadirachta indica and Carapa procera(Meliaceae) seed oils and cakes obtained after oil extraction, Ind. Crops Prod., 38, 39-45 (2012) @No $ @ @ Faye M., Nouveau procédé de fractionnement de la graine de neem (Azadirachta indica A. Juss) sénégalais: production d’un biopesticide d’huile et de tourteau, Thèse en Sciences des Agroressources, Université de Toulouse (2010) @No $ @ @ Addea-Mensah I., The uses of the neem (Azadirachta indica) in Ghana and their relations of the chemical constituents and biological activities, Proc. Seminar held Dodowa: the potentials of the neem trees in Ghana, 11-26 (1998) @No $ @ @ Djenontin Tindo S., Amusant N., Dangou J., Wotto D.V., Avlessi F., Dahouénon-Ahoussi E., Lozano P., Pioch D. and Sohounhloué K.C.D., Screening of repellent, termiticidal and preventive activities on wood, of Azadirachta indica and Carapa procera (Meliaceae) seeds oils, ISCA J. Biological Sci., 1(3), 25-29 (2012) @No $ @ @ Zongo J.O., Vincent C. and Stewart R.K., Effects of neem seed kernel extracts on egg and larval survival of the sorghum shoot fly, Atherigona soccata Rondani (Dipt.: Muscidae), J. Appl. Entomol., 115, 363-369 (1993) @No $ @ @ Jadeja G.C., Maheshwari R.C. and Naik S.N., Extraction of natural insecticide azadirachtin from neem Azadirachta indica A.Juss) seed kernels using pressurized hot solvent, J. of Supercritical Fluids., 56, 253-258 (2011) @No $ @ @ Saxena M., Ravikanth K., Kumar A., Gupta A., Singh B. and Sharma A., Purification of Azadirachta indica seed cake and its impact on nutritional and antinutritional factors, J. Agric. Food Chem., 58, 4939-4944 (2010) @No $ @ @ Debashri M. and Tamal M., A Review on efficacy of Azadirachta indica A, Juss based biopesticides: An Indian perspective, Res. J. Recent Sciences, 1(3), 94-99 (2012) @No $ @ @ Sharma D.K. and Ansari B.A., Toxicity of azadirachtin on some biomarkers of oxidative stress in zebrafish, Daniorerio, J. Biol. and Earth Sciences, 4(2), B160-B167 (2014) @No $ @ @ Haidara A.O., Valorisation d’une huile végétale tropicale: l’huile de pourghère,  Mémoire Maitrise Université de Sherbrooke, Canada (1996) @No $ @ @ Van Soest P.J. and Wine R.H., Determination of lignin and cellulose in acid detergent fiber with permanganate, J. Am. Oil Chem. Soc., 51(4), 780-784 (1968) @No $ @ @ Martin C., Moure A., Giraldo Martin G., Carrillo E., Dominguez H. and Parajo J.C., Fractional characterisation of Jatropha, neem, Moringa, Trisperma, castor and candlenut  seeds as potential feedstocks for biodiesel production in Cuba, Biomass and Bioenergy, 34, 533-538 (2010) @No $ @ @ Ghedira K., Les flavonoïdes: structure, propriétés biologiques, rôle prophylactique et emplois phytothérapeutique, Phytothérapie., , 162-169 (2005) @No $ @ @ Vaitillingom G., Utilisations énergétiques de l’huile de coton, Cahiers Agricultures., 15 (1), 144-149 (2006) @No $ @ @ Musa U. and Folorusho A., Characteristics of a typical Nigerian Jatrophacurcas oil seeds for biodiesel production, Res. J. Chem. Sci., 2(10), 7-12 (2012) @No $ @ @Djenontin S.T., Dangou J., Wotto D.V., Sohounhloué K.C.D., Lozano P. and Pioch D., Composition en acides gras, stérols et tocophérols de l’huile végétale non conventionnelle extraite des graines de Jatropha curcas(Euphorbiaceae) du Bénin, . Soc. Ouest-Afr. Chim., 22, 59-68 (2006) @No $ @ @ Kritchevsky D. and Shirley C.C., Phytosterols health benefits and potential concerns: a review, Nutrition Res., 25, 413-428 (2005) @No $ @ @ Feinberg M., Favier J.C. and Ireland-Ripert J., Répertoire général des aliments. In: Tables de Composition des Corps Gras, Lavoisier-Tec and Doc, INRA Editions, Paris (1987) @No $ @ @ Nonviho G., Paris C., Muniglia L., Sessou P., Agbangnan D.C.P., Brosse N. and Sohounhloué D., Chemical characterization of Lophiralanceolata and Carapaprocera seed oils: analysis of fatty acids, sterols, tocopherols and tocotrienols, ISCA Res. J. Chem. Sci., 4(9), 57-62 (2014) @No $ @ @ Awad A.B., Chan K.C., Downie A.C. and Fink C.S., Peanuts as a source of -sitosterol, a sterol with anticancer properties, Nutr. Cancer, 36, 238-241 (2000) @No $ @ @ Demir C. and Cetin M., Determination of tocopherols, fatty acids and oxidative stability of pecan, walnut and sunflower oils, Deutsche Lebensmittel-Rundschau., 95, 278-282 (1999) @No $ @ @ Bramley P.M., Elmafda I., Kafatos A., Kelly F.J., Manios Y., Roxborough H.E., Schuch W., Sheehy P.J.A. and Wagner K.H., Vitamin E, J. Sci. Food Agri., 80, 913-938 (2000) @No